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Non-catalytic pyrolysis of scrap tires using a newly developed two-stage pyrolyzer for the production of a pyrolysis oil with a low sulfur content

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  • Choi, Gyung-Goo
  • Oh, Seung-Jin
  • Kim, Joo-Sik
Abstract
The aim of this work was to reduce the sulfur content of pyrolysis oil derived from the scrap tire pyrolysis. In this respect, a series of pyrolysis experiments was conducted in both a fluidized bed reactor (one-stage pyrolysis) and a newly developed two-stage pyrolyzer consisting of an auger reactor and a fluidized bed reactor in series (two-stage pyrolysis). The one-stage pyrolysis was carried out at ∼500 and 600°C with different fluidizing gases (N2 and product gas). In the experiments, the pyrolysis oil obtained at ∼500°C had a lower sulfur content than that produced at ∼600°C. N2 was better at producing a low-sulfur pyrolysis oil than product gas. The sulfur contents of the oils obtained from the one-stage pyrolysis ranged from 0.75 to 0.92wt.%. The two-stage pyrolysis was conducted using product gas as the fluidizing medium at different auger reactor temperatures (∼230–450°C) and at a constant fluidized bed reactor temperature (∼510°C). A pyrolysis oil containing only 0.55wt.% of sulfur could be produced at the temperatures of the auger reactor of ∼330°C and fluidized bed reactor of ∼510°C. Moreover, the two-stage pyrolysis could produce an oil with a low nitrogen content (0.28wt.%). A pyrolysis oil obtained from the auger reactor contained dl-limonene up to 50wt.%.

Suggested Citation

  • Choi, Gyung-Goo & Oh, Seung-Jin & Kim, Joo-Sik, 2016. "Non-catalytic pyrolysis of scrap tires using a newly developed two-stage pyrolyzer for the production of a pyrolysis oil with a low sulfur content," Applied Energy, Elsevier, vol. 170(C), pages 140-147.
    • Handle: RePEc:eee:appene:v:170:y:2016:i:c:p:140-147
    DOI: 10.1016/j.apenergy.2016.02.119
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    References listed on IDEAS

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    1. Martínez, Juan Daniel & Puy, Neus & Murillo, Ramón & García, Tomás & Navarro, María Victoria & Mastral, Ana Maria, 2013. "Waste tyre pyrolysis – A review," Renewable and Sustainable Energy Reviews, Elsevier, vol. 23(C), pages 179-213.
    2. Martínez, Juan Daniel & Ramos, Ángel & Armas, Octavio & Murillo, Ramón & García, Tomás, 2014. "Potential for using a tire pyrolysis liquid-diesel fuel blend in a light duty engine under transient operation," Applied Energy, Elsevier, vol. 130(C), pages 437-446.
    3. Antoniou, N. & Zabaniotou, A., 2013. "Features of an efficient and environmentally attractive used tyres pyrolysis with energy and material recovery," Renewable and Sustainable Energy Reviews, Elsevier, vol. 20(C), pages 539-558.
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    Cited by:

    1. Choi, Gyung-Goo & Oh, Seung-Jin & Kim, Joo-Sik, 2016. "Scrap tire pyrolysis using a new type two-stage pyrolyzer: Effects of dolomite and olivine on producing a low-sulfur pyrolysis oil," Energy, Elsevier, vol. 114(C), pages 457-464.
    2. Alexander A. R. Gamboa & Leila R. dos Santos & Cristiane A. Martins & Ana M. A. Rocha & Carlos A. Alvarado-Silva & João A. de Carvalho, 2023. "Thermodynamic Evaluation of the Energy Self-Sufficiency of the Tyre Pyrolysis Process," Energies, MDPI, vol. 16(24), pages 1-26, December.
    3. Sophonrat, Nanta & Sandström, Linda & Zaini, Ilman Nuran & Yang, Weihong, 2018. "Stepwise pyrolysis of mixed plastics and paper for separation of oxygenated and hydrocarbon condensates," Applied Energy, Elsevier, vol. 229(C), pages 314-325.
    4. Czajczyńska, Dina & Krzyżyńska, Renata & Jouhara, Hussam & Spencer, Nik, 2017. "Use of pyrolytic gas from waste tire as a fuel: A review," Energy, Elsevier, vol. 134(C), pages 1121-1131.
    5. Choi, Gyung-Goo & Oh, Seung-Jin & Kim, Joo-Sik, 2017. "Clean pyrolysis oil from a continuous two-stage pyrolysis of scrap tires using in-situ and ex-situ desulfurization," Energy, Elsevier, vol. 141(C), pages 2234-2241.
    6. Park, Ki-Bum & Jeong, Yong-Seong & Guzelciftci, Begum & Kim, Joo-Sik, 2019. "Characteristics of a new type continuous two-stage pyrolysis of waste polyethylene," Energy, Elsevier, vol. 166(C), pages 343-351.
    7. Arabiourrutia, Miriam & Lopez, Gartzen & Artetxe, Maite & Alvarez, Jon & Bilbao, Javier & Olazar, Martin, 2020. "Waste tyre valorization by catalytic pyrolysis – A review," Renewable and Sustainable Energy Reviews, Elsevier, vol. 129(C).
    8. Campuzano, Felipe & Brown, Robert C. & Martínez, Juan Daniel, 2019. "Auger reactors for pyrolysis of biomass and wastes," Renewable and Sustainable Energy Reviews, Elsevier, vol. 102(C), pages 372-409.
    9. Amir Rowhani & Thomas J. Rainey, 2016. "Scrap Tyre Management Pathways and Their Use as a Fuel—A Review," Energies, MDPI, vol. 9(11), pages 1-26, October.
    10. Alvarez, J. & Lopez, G. & Amutio, M. & Mkhize, N.M. & Danon, B. & van der Gryp, P. & Görgens, J.F. & Bilbao, J. & Olazar, M., 2017. "Evaluation of the properties of tyre pyrolysis oils obtained in a conical spouted bed reactor," Energy, Elsevier, vol. 128(C), pages 463-474.
    11. Cho, Seong-Heon & Oh, Jeong-Ik & Jung, Sungyup & Park, Young-Kwon & Tsang, Yiu Fai & Ok, Yong Sik & Kwon, Eilhann E., 2020. "Catalytic pyrolytic platform for scrap tires using CO2 and steel slag," Applied Energy, Elsevier, vol. 259(C).
    12. Zhao, Xinyue & Chen, Heng & Li, Sarengaowa & Li, Wenchao & Pan, Peiyuan & Liu, Tao & Wu, Lining & Xu, Gang, 2023. "Thermodynamic and economic analysis of a novel design combining waste tire pyrolysis with silicon production waste heat recovery and organic Rankine cycle," Energy, Elsevier, vol. 283(C).

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